2,2′-Hexamethylenedi-1,3-benzothiazole
نویسندگان
چکیده
The title compound, C(20)H(20)N(2)S(2), was prepared by the reaction of suberic acid and 2-amino-thio-phenol under microwave irradiation. The mol-ecule lies on an inversion center.
منابع مشابه
catena-Poly[[(2-amino-1,3-benzothiazole-6-carboxylato-κ2 O,O′)(2,2′-bipyridyl-κ2 N,N′)cadmium]-μ-2-amino-1,3-benzothiazole-6-carboxylato-κ3 N 1:O,O′]
In the title coordination polymer, [Cd(C(8)H(5)N(2)O(2)S)(2)(C(10)H(8)N(2))](n), the Cd(II) ion is coordinated by a bidentate 2,2-bipyridyl ligand, two O,O'-chelating 2-amino-1,3-benzothia-zole-6-carboxyl-ate (ABTC) ligands and one N-bonded ABTC ligand. The resulting CdN(3)O(4) coordination polyhedron approximates to a very distorted penta-gonal bipramid with one O and one N atom in axial posit...
متن کامل2-[3-(1,3-Benzothiazol-2-yl)-2,2-dimethylpropyl]-2-methyl-2,3-dihydro-1,3-benzothiazole
In the title compound, C(20)H(22)N(2)S(2), the five-membered thia-zole ring of the 2-methyl-2,3-dihydro-1,3-benzothia-zole unit has an envelope conformation. The dihedral angle between the planar [maximum deviation of 0.014 (1) Å for the S atom] benzothia-zole ring system and the benzene ring is 78.37 (12)°. Two intra-molecular C-H⋯S hydrogen bonds are observed, forming rings of graph-set motif...
متن کامل2,2′-(Sulfanediyldimethylene)bis(1,3-benzothiazole)
In the title compound, C(16)H(12)N(2)S(3), the two benzothia-zole groups are oriented differently with respect to the -CH(2)- groups, one being approximately staggered and one nearly eclipsed. A sulfur-π inter-action of 3.3627 (11) Å is observed between the bridging thio-ether S atom and a thia-zole ring. The crystal packing is further stabilized by inter-molecular C-H⋯N and C-H⋯π inter-actions.
متن کامل4′-tert-Butyl-5-chloro-3H-spiro[1,3-benzothiazole-2,1′-cyclohexane]
In the title compound, C(16)H(22)ClNS, the nine-membered 2,3-dihydro-1,3-benzothia-zole ring system is essentially planar, with a maximum deviation of 0.025 (2) Å for the N atom. Its plane is almost perpendicular to the main plane of the substituted cyclo-hexane ring, which adopts a chair conformation. In the crystal, the molecules are linked by C-H⋯π inter-actions.
متن کامل2-Amino-6-methyl-1,3-benzothiazole–octanedioic acid (2/1)
Cocrystallization of 2-amino-6-methy-1,3-benzothia-zole with octa-nedioic acid in a mixed methanol-water medium afforded the title 2:1 cocrystal, 2C(8)H(8)N(2)S·C(8)H(14)O(4). The octa-nedioic acid mol-ecule is located on an inversion centre. In the crystal, inter-molecular N-H⋯O and O-H⋯O hydrogen bonds connect the components into a three-dimensional network.
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عنوان ژورنال:
دوره 65 شماره
صفحات -
تاریخ انتشار 2009